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1 article(s) from Eyers, Claire E

Formation of carbohydrate-functionalised polystyrene and glass slides and their analysis by MALDI-TOF MS

Martin J. Weissenborn,
Johannes W. Wehner,
Christopher J. Gray,
Robert Šardzík,
Claire E. Eyers,
Thisbe K. Lindhorst and
Sabine L. Flitsch

Beilstein J. Org. Chem. 2012, 8, 753–762, doi:10.3762/bjoc.8.86

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Figure 1: Carbohydrate arrays on polystyrene slides can be obtained by noncovalent immobilisation of tritylat...

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Scheme 1: Synthesis of the tritylated compounds 3 [28], 5 and 7: (a) dichloromethane, 2.5 h, rt, 98%, (b) HBTU/DI...

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Figure 2: Comparison of the polystyrene and glass surfaces with and without aluminium backing by matrix-free ...

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Scheme 2: The Man–Trt compound 5 forms the disulfide 8 during UV ionisation in MALDI-TOF MS analysis.

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Figure 3: Limit-of-detection analysis of 5 on aluminium-backed glass and polystyrene slides. Both systems sho...

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Figure 4: Comparison of MALDI-TOF MS spectra on the aluminium-backed polystyrene and glass slides after washi...

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Figure 5: Photo of the aluminium strip on the back of the polystyrene support.

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Published 21 May 2012

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